ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India – Download as PDF File .pdf), Text File .txt) or read online. ASTM A Practice A test (Oxalic acid test). The oxalic acid etch test is rapid and nondestructive, but not quantitative. It is a rapid etching procedure and . Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. This abstract is a brief summary of the referenced standard. Link to Active This link will always route to the current Active version of the standard.
At the conclusion off the test, specimens are either visually examined or measured for weight ast and compared to an established corrosion rate for that specific material type. Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries.
Intergranular Corrosion Testing: An Overview of ASTM A262
Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack. The inch-pound equivalents are in parentheses practiice may be approximate. In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.
The samples are etched after metallographic preparation for cross-sectional examination which is thoroughly viewed with a traverse from inside to outside diameters of rods and tubes, from face to face on plates, and across all zones such as weld metal, weld-affected zones, and base plates on specimens containing welds.
These practices include five intergranular corrosion tests, namely: Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges.
Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.
Practice E, the Strauss test, is performed to assess attack associated wstm chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. The test uses a visual inspection of the surface of the bent specimen to determine pass or fail. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
Like what you saw? The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack.
This test aatm used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.
G2MT Practics is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed. This practice includes boiling the sample for w to hours in the solution above, and measures the materials performance quantitatively.
Intergranular corrosion shows up as the dark black lines around the grain boundaries. ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results.
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
Since practiec temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.
From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
Classification praxtice structure then provides either acceptance or further testing required, which typically moves you to one of the next practices. Carbon and Sulfur Analysis. It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries. Intergranular corrosion is the proper use, though the specification calls it attack, corrosion is what is taking place.
Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA.
If the structure is acceptable no additional testing is required. This method is preferable for chromium depletions and corrosion in intermetallic phases. Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: What is your typical turnaround time? Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of astk to rapid intergranular attack.
We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to practuce environments.
ASTM A Intergranular Corrosion Testing and Analysis
The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions.
If materials with incorrect heat treatment enter service, they are liable to crack or fail x262 intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed. A different ASTM A aetm method must be used to quantify the level of corrosion or to disqualify a material for use. Historical Version s – view previous versions of standard.